NO.

氨基酸名称

AA Code

MW

CAS

熔点值

旋光值(MERK)

旋光值

1

Fmoc-Arg(pbf)

-OH

R

648.77

154445-77

-9

132

-9.0--3.0°

c=1

in DMF

-6±3°

c=1

in DMF

2

Fmoc-Cys(Trt)

-OH

C

585.44

103213-32

-7

171-174

+17.5-+22.5°

c=1

in DMF

+16.0±2°

c=1

in tetrahydrofuran

3

Fmoc-Glu(Otbu)-OH

E

425.47

71989-18-9

83-90

-10.0--7.0°

c=1

in MeOH

-4.5±1°

c=1

in HAc:water4:1

4

Fmoc-Gly

-OH

G

297.31

29002-11-5

174-178

5

Fmoc-Ala-OH

A

311.3

35661-39-3

147-153

-20.5--15.5°

c=1

in DMF

-18°

c=1

in DMF

6

Fmoc-Asn(Trt)-OH

N

596.67

132388-59

-1

210-214

-16.5--12.5°c=1

in MeOH

-15.0±1°

c=1

in MeOH

7

Fmoc-His(Trt)

-OH

H

619.71

109425-51

-6

150－155

+87-+97°

c=5%

in CHCl3

+92±5°

c=5%

in CHCl3

8

Fmoc-Ile-OH

I

353.41

71989-23-6

146-149

-14--10°

c=1

in DMF

-12±1°

c=1

in DMF

9

Fmoc-Leu-OH

L

353.41

35661-60-0

152-156

-8.5--5.5°

c=1

in EtOAc

-25±2°

c=1

in DMF

10

Fmoc-Asp(Otbu)-OH

D

411.45

71989-14-5

148-150

(dec)

-26.5--21.5°

c=1

in DMF

-24±2°

c=1

in DMF

11

Fmoc-Val-OH

V

339.39

68858-20-8

143-147

-18.5--14.5°

c=1

in DMF

-17±1°

c=1

in DMF

12

Fmoc-Tyr(tBu)

-OH

Y

459.53

71989-38-3

～150

(dec)

-31.3--26.0°

c=1

in DMF

-29±2°

c=1

in DMF

13

Fmoc-Thr(tBu)

-OH

T

397.46

71989-35-0

131-134

13.0-+17.0°

c=1

in EtOAc

+16±1°

c=1

in EtOAc

14

Fmoc-Ser(tBu)-OH

S

383.44

71989-33-8

～130

+22.5-+27.5°

c=1

in EtOAc

+25.5±1°

c=1

in EtOAc

15

Fmoc-Phe-OH

F

387.43

35661-40-6

180-187

-40.5--35.5°

c=1

in DMF

-37°

c=1

in DMF

16

Fmoc-Lys(Boc)-OH

K

468.54

71989-26-9

130-135

-12.5--9.5°

c=1

in DMF

-12±1°

c=1

in DMF

17

Fmoc-Met

-OH

M

371.45

71989-28-1

121-123

-30.5--26.5°

c=1

in DMF

-30±1°

c=1

in DMF

18

Fmoc-Gln(Trt)-OH

Q

610.71

132327-80

-1

165-172

-2.4--0.4°

c=1

in MeOH

-14.0±1.5°

c=1

in DMF

19

Fmoc-Pro

-OH

P

337.37

71989-31-6

117-118

-34.5--29.5°

c=1

in DMF

-32±1°

c=1

in DMF

20

Boc-Lys(Fmoc)-OH

K

468.54

84624-27-1

?

+3.3±0.5°

c=1

in EtOAc

+3.0-+5.0°

c=1

in EtOAc